Disputation: Valmir Rodrigo da Silva

Doctoral candidate Valmir Rodrigo da Silva at the Chemistry Department, Faculty of Mathematics and Natural Sciences, is defending the thesis Synthesis and Characterization of Iron Nickel-based alloys for rare earth-free permanent magnet applications for the degree of Philosophiae Doctor.

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Valmir Rodrigo da Silva

The Disputation will be live streamed for everyone else.
The livestream will be activated 15 minutes before the Defense starts.

Trial lecture

May 07, 10:15 Auditorium 2, Chemistry Building

Trial lecture title: “Recycling of Nd-Fe-B Permanent Magnets” 

 

Conferral summary / Kreeringssammendrag

Denne forskningen utforsket metoder for å fremstille tetrataenitt kunstig, en bærekraftig jern-nikkel-legering som kan erstatte dyre magneter av sjeldne jordmetaller i grønn teknologi. Ved å kontrollere de strukturelle defektene som oppstår under fremstillingen, undersøkte dette arbeidet viktige kinetiske barrierer og la et avgjørende grunnlag for fremtidig produksjon av disse strategiske og potensielt høytytende magnetene.

Main research findings

This research provides critical insights into synthesizing tetrataenite, a meteorite-derived iron-nickel alloy that could replace expensive rare-earth permanent magnets in green technologies.

And to artificially produce this material, I used mechanical activation techniques, such as cryomilling and cold rolling, and added elements such as carbon, molybdenum, and aluminium. These methods aimed to increase atomic mobility and speed up the slow atomic ordering process. We followed this with long-term heat treatment (annealing) at a temperature just below the alloy’s order-disorder transition temperature (estimated to be around 320 °C).

But, perfectly recreating the highly ordered atomic structure of tetrataenite in bulk form proved exceptionally challenging, and it could not be definitively confirmed in the studied samples.

Therefore, I focused on understanding the precise microscopic changes that occur during these manufacturing attempts. I successfully identified the formation of specific structural imperfections, known as planar defects (such as stacking faults and twinning), in the processed materials. By evaluating how these microscopic defects and chemical additions influence the iron-nickel structure, my findings decode key kinetic barriers, laying essential groundwork for producing sustainable, high-performance permanent magnets.

Candidate contact information

E: mail: valmir.silva@ife.no 
Telephone: +47 922 57 207

Adjudication committee

Scientific Group Leader Dr. Thomas George Woodcock 
Leibniz Institute for Solid State and Materials Research, Dresden, Germany

Senior Professional Research Associate Petra Jenuš Belec
Jožef Stefan Institute, Ljubljana, Slovenia

Postdoctoral Researcher Ken Luca Abel
Centre for Materials Science and Nanotechnology, University of Oslo, Norway

Chair of defence

Professor Unni Olsbye, Department of Chemistry, University of Oslo

Supervisors

Head of Research Bjørn C. Hauback, Department of Chemistry, University of Oslo

Senior Scientist Stefano Deledda, Ife, Norway

Professor Emeritus Helmer Fjellvåg, Department of Chemistry, University of Oslo

Scientist Christoph Frommen, Ife, Norway

 

Published Apr. 23, 2026 4:20 PM - Last modified May 7, 2026 12:39 PM